数字式定温热偶真空计

本文介绍了一种新的数字式定温热偶真空计，它具有精度高、工作可靠、结构简单、操作方便等优点。文中具体阐述了微机系统的工作原理，并提供了结构原理框图。概述了研制中的关键技术问题，即用微机软件对非线性进行补偿的方法。最后介绍了该真空计的主要算法及应用实例。     

非无线电设备的无线电波辐射

介绍了电磁辐射的分类和非无线电辐射造成的各种危害，指出了可能产生电磁辐射的设备，给出了几种特殊情况的辐射值，并结合国际标准和国家标准，分析了电磁干扰的管理现状，最后提出了减少非无线电设备电磁辐的几种方法。     

聚合物分解法制备微波介质陶瓷粉体的研究

对采用聚合物分解（Ｐｅｃｈｉｎｉ）法制备ＭｇＴｉＯ＿３粉体进行了研究。通过对聚合中间产物进行红外光谱分析，研究了聚合物分解法制备ＭｇＴｉＯ＿３陶瓷粉体的聚合反应过程及产物。并与用传统固相反应法制备粉体工艺进行对比．从而证明用聚合物分解法可获得单一ＭｇＴｉＯ＿３相材料．并可降低粉体的煅烧温度。     

甲状腺素T4免疫传感器的研究

报道以甲基丙烯酸羟乙酯与甲基丙烯酸甲酯的共聚物为载体膜材料，研制成非酶标记的Ｔ４免疫传感器，并对载体膜材料的共聚方法及共聚物共聚比与传感器灵敏度的关系进行了探讨。     

Ultrasonic thin-walled tube wave structure for sensing devices

Theoretical and experimental investigations of thin-walled tube acoustic wave devices for gravimetric sensing applications are presented. Integrated sensor configurations have been demonstrated by employing a sol-gel processed thin piezoelectric lead zirconate titanate (PZT) film. This was coated coaxially on stainless steel tubes and interdigital transducers (IDT) fabricated as the transmitter and receiver on the curved tube surfaces. We have observed tube waves along both the axial and circumferential directions between 1 and 6.6 MHz. We have also analyzed the mass sensitivities of different modes propagating along the tubes and shown that high mass sensitivity can be achieved by keeping the tube wall thin     

加强行业技术管理推动材料技术进步

论述了制定《航空工业材料及热工艺技术工作规定》的必要性和航空材料及热工艺的内涵及其重要性，提出确保航空产品质量是航空材料及热工艺技术管理工作的永恒主题，而加强和健全航空材料及热工艺技术管理机构，完善其规章制度则是保证航空产品质量的重要措施，该机构的主要职责是技术立法、技术发展和技术归口。     

Stabilization of wave equations coupled in parallel by viscous damping

In this article, we consider stabilization of two wave equations coupled in parallel by viscous damping. Uniform exponential stabilization can be achieved when damping is presented in two equations. In general only strong stabilization can be achieved when damping is present in one equation, while uniform exponential stabilization is still possible for some special cases.     

Stability of Mixtoxantrone Hydrochloride in Solution

A stability-indicating reversed-phase high performance liquid chromatographic method was developed for the detection of mitoxantrone HC1 and its degradation products under accelerated degradation conditions. The degradation kinetics of mitoxantrone HC1 in aqueous solution over a pH range of 1.18 to 7.20 and its stability in propylene glycol-or polyethylene glycol 400-based solutions were investigated. The observed rate constants were shown to follow apparent first-order kinetics in all cases. The pH-rate profile shows that maximum stability of mitoxantrone HC1 was obtained at pH 4.01. No general acid or base catalysis from acetate or phosphate buffer species was observed. The catalysis rate constants on the protonated mitoxantrone imposed by hydrogen ion water and hydroxy ion were determined to be 3.72 × 10 min^-1 5.64 × 10-min^-1 and 1.108 × 10^-2min^-1, respectively. The degradation rate constants of mitoxantrone affected by different ionic strength systems. Irradiation with 254 nm UV light at 25±0.5°C was found when canpared with the light-protected controls. Incorporation of nonaqueous propylene glycol or polyethylene glycol in the pH 4.01 mitoxantrone solution shows an increase in its stability at 502±0.5°C.     

用热分析法研究硝化棉的熔化过程

用ＭＤＳＣ，显微镜温台熔点测定仪和固体原位反应池／快速扫描傅立叶变换红外光谱联用装置考察了硝化棉的熔化过程。ＭＤＳＣ曲线表明吸热过程是可逆的，它系由ＮＣ和部分分解凝聚相产物的混合物的固液相变所引起。由ＮＣ的ＭＤＳＣ曲线得到的熔点，熔化含，熔化熵，分解含和分解反应热温熵分别为４７６．８４Ｋ，２０５．６Ｊ．ｇ＾－１，０．４３１２Ｊ．ｇ＾－１．Ｋ＾－１，－２４７５．０Ｊ．ｇ＾－１，－５．２４２Ｊ．ｇ＾－